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1 M), for 48 hours

S(CAM- d 15 TPP) 2 , dichloride salt A solution of 5-aminopentyltripentadeuterotriphenylphosphonium bromide hydrogen bromide (102 mg, 0.2 mmol, prepared as for SS(CAM- d 15 TPP) 2 above), 2,2-thiodiacetic (15 mg, 0.1 mmol), HBTU (90 mg, 0.22 mmol) and DIPEA (0.07 mL, 0.4 mmol) in anhydrous DMF (1.0 mL) was stirred under argon for 1 h