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a, b, c, d, e, f Brus, D.: Spatial Sampling with R, Chapman & Hall/CRC The R Series, CRC Press, Boca Raton, ISBN 9781000600056, 2022

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Samples were concentrated to dryness in vacuum before dissolving in 150 L 80% methanol solution, then centrifuged again at 13 500 g and 4C for 10 min, and the supernatant was transferred to a new tube for LC-MS detection

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